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Se2NCl3 and [Se2NCl2]+ [GaCl4]−, Chloride Nitrides of Trivalent Selenium

✍ Scribed by Dr. René Wollert; Dipl.-Chem. Antje Höllwarth; Prof. Dr. Gernot Frenking; Prof. Dr. Dieter Fenske; Dr. Helmut Goesmann; Prof. Dr. Kurt Dehnicke

Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
359 KB
Volume
31
Category
Article
ISSN
0044-8249

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Ruby-red, bead-shaped single crystals of C-type La 2 Se 3 (a = 905.21(6) pm), Pr 2 Se 3 (a = 891.17(6) pm), and Gd 2 Se 3 (a = 872.56(5) pm) are obtained by oxidation of the respective rare-earth metal (M = La, Pr and Gd) with selenium (molar ratio 2 : 3) in evacuated silica tubes at 750 °C in the p