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Scanning Electron Microscopy and X-Ray Microanalysis: A Text for Biologists, Materials Scientists, and Geologists

✍ Scribed by Joseph I. Goldstein, Dale E. Newbury, Patrick Echlin, David C. Joy, A. D. Romig Jr., Charles E. Lyman, Charles Fiori, Eric Lifshin (auth.)


Publisher
Springer US
Year
1992
Tongue
English
Leaves
829
Edition
2
Category
Library

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✦ Synopsis


In the last decade, since the publication of the first edition of Scanning Electron Microscopy and X-ray Microanalysis, there has been a great expansion in the capabilities of the basic SEM and EPMA. HighΒ­ resolution imaging has been developed with the aid of an extensive range of field emission gun (FEG) microscopes. The magnification ranges of these instruments now overlap those of the transmission electron microscope. Low-voltage microscopy using the FEG now allows for the observation of noncoated samples. In addition, advances in the developΒ­ ment of x-ray wavelength and energy dispersive spectrometers allow for the measurement of low-energy x-rays, particularly from the light elements (B, C, N, 0). In the area of x-ray microanalysis, great advances have been made, particularly with the "phi rho z" [Ij)(pz)] technique for solid samples, and with other quantitation methods for thin films, particles, rough surfaces, and the light elements. In addition, x-ray imaging has advanced from the conventional technique of "dot mapping" to the method of quantitative compositional imaging. Beyond this, new software has allowed the development of much more meaningful displays for both imaging and quantitative analysis results and the capability for integrating the data to obtain specific information such as precipitate size, chemical analysis in designated areas or along specific directions, and local chemical inhomogeneities.

✦ Table of Contents


Front Matter....Pages i-xviii
Introduction....Pages 1-19
Electron Optics....Pages 21-68
Electron-Specimen Interactions....Pages 69-147
Image Formation and Interpretation....Pages 149-271
X-Ray Spectral Measurement: WDS and EDS....Pages 273-339
Qualitative X-Ray Analysis....Pages 341-364
X-Ray Peak and Background Measurements....Pages 365-393
Quantitative X-Ray Analysis: The Basics....Pages 395-416
Quantitative X-Ray Analysis: Theory and Practice....Pages 417-523
Compositional Imaging....Pages 525-545
Specimen Preparation for Inorganic Materials: Microstructural and Microchemical Analysis....Pages 547-570
Sample Preparation for Biological, Organic, Polymeric, and Hydrated Materials....Pages 571-670
Coating and Conductivity Techniques for SEM and Microanalysis....Pages 671-740
Data Base....Pages 741-785
Back Matter....Pages 787-820

✦ Subjects


Earth Sciences, general; Developmental Biology; Characterization and Evaluation of Materials


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