The magic-angle spinning sidebands of the satellite transition (ST, m = +/- 3/2 <==> +/- 1/2) for 11B nuclear magnetic resonance (11B ST spectroscopy) have been used to detect multiple boron sites in Na2O-B2O3-SiO2 glasses. The experimental details and data analysis are described, how multiple BO4 a
Satellites and shoulders in the NMR 11B resonance of borate glass
β Scribed by P.W France; M Wadsworth
- Publisher
- Elsevier Science
- Year
- 1982
- Weight
- 505 KB
- Volume
- 49
- Category
- Article
- ISSN
- 0022-2364
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π SIMILAR VOLUMES
Glasses in the system xB 2 O 3 Γ Γ°1 Γ xΓSiO 2 Γ°0:2 x 1:0Γ were studied using 11 B multiple quantum magic angle spinning NMR spectroscopy (MQMAS), 29 Si-f 11 Bg rotational echo adiabatic passage double-resonance and 29 Si-f 11 Bg CP heteronuclear correlation spectroscopy. The results can be quantita
The formation of borate esters of various mono-and di-saccharides in aqueous solution was studied by "B and 13C NMR spectroscopy. Association constants K(B-L) at a carbohydrate-borate molar ratio of 1: 1, pH 7, and 25Β°C were determined and compared with literature values obtained from potentiometry.
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