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(S)-2-(Pyrrolidinium-2-ylmethyl)isoquinolinium dibromide

✍ Scribed by Wang, Bing-Tao ;Luo, Shu-Ping ;Yue, Hua-Dong ;Wang, Li-Ping ;Xu, Dan-Qian

Book ID
104490827
Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
563 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the crystal structure of the title compound, C 14 H 18 N 2 + Á2Br À , molecules are linked by N-HÁ Á ÁBr hydrogen bonds.

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In the title compound, C~11~H~18~N~2~ ^2+^·2Br^−^, whose cation represents the product of racemization of an L-proline derivative under basic conditions, the pyrrolidinium ring has a distorted envelope conformation with the N atom deviating by 0.533 (6) Å from the mean plane of the remaining four at

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✍ Eirik Sundby; Jarle Holt; Anders Vik; Thorleif Anthonsen 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 106 KB

## Abstract Lipase‐catalyzed transesterifications and biological reductions were used to obtain the (__S__)‐enantiomers of 3‐chloro‐1‐(1,3‐dithian‐2‐yl)‐2‐propanol and 1‐(1,3‐dithian‐2‐yl)‐3‐fluoro‐2‐propanol and their (__R__)‐acetates. (__S__)‐3‐Chloro‐1‐(1,3‐dithian‐2‐yl)‐2‐propanol and (__R__)‐3