(RS)-1 4-Dibenzoyl-cis-2,5-dimethylpiperazine
✍ Scribed by Sakurai, T. ;Nakamaru, M. ;Tsuboyama, S. ;Tsuboyama, K.
- Book ID
- 114524640
- Publisher
- International Union of Crystallography
- Year
- 1977
- Weight
- 344 KB
- Volume
- 33
- Category
- Article
- ISSN
- 0567-7408
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The title compound, C 34 H 28 O 3 S 2 , was synthesized by the reaction of thiophene-2-carbaldehyde with acetophenone and NaOH under phase-transfer catalysis and solvent-free conditions. The central six-membered ring adopts a chair conformation and all the bulky side groups are located in equatorial
In this paper, we present the crystal structure of 2,4-Dibenzoyl-1,3,5-triphenyl-1-cyclohexanol (I) dichloromethane 2:1 solvate, which was synthesized through the condensation and Micheal addition of benzaldehyde with acetophenone under tetrabutyl ammonium bromide and solvent-free conditions. In th