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Ring-size effects in the reaction of benzocycloalkadiene epoxides with lithium diisopropylamide

✍ Scribed by Thies, Richard W.; Chiarello, Ronald H.

Book ID
127320126
Publisher
American Chemical Society
Year
1979
Tongue
English
Weight
416 KB
Volume
44
Category
Article
ISSN
0022-3263

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## 2,4-Di-t-butyl-6-methylphenylphosphonous dichloride reacted with chloroform in the presence of lithium diisopropylamide to give (2,4-di-t-butyl-6-methylphenyl) (dichloromethyl) ( I , 2,2-trichloroethenyl)phosphine. The structure of this phosphine was analyzed by X-ray crystallography. This phosph