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Ring-Opening of N-Lithio-2,3(cis)-diphenylaziridine to 1,3(cis, trans)-Diphenyl-2-azaallyllithium and Its Rearrangement to the trans, trans-Form

✍ Scribed by Prof. Dr. Thomas Kauffmann; Dipl.-Chem. Kai Habersaat; Dr. Edgar Köppelmann


Publisher
John Wiley and Sons
Year
1972
Tongue
English
Weight
235 KB
Volume
11
Category
Article
ISSN
0044-8249

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The analysis (separation and identification) of eleven C,H,, isomers is performed using coupled GC/MS with a 70 m glass capillary column containing a 2.5 pm thick film of P a 2 5 as stationary phase. Cryogenic €20, cooling improves the separations. The total analysis time is lees than 12 minutes. S