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Ring inversion barriers of 1,4-dioxane and cis-2,3-dimethyl-1,4-dioxane. Carbon-13 coupling-induced nonequivalence of vicinal protons

✍ Scribed by Jensen, Frederick R.; Neese, Richard A.

Book ID
127186103
Publisher
American Chemical Society
Year
1975
Tongue
English
Weight
431 KB
Volume
97
Category
Article
ISSN
0002-7863

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On the stereochemistry of 1,4-diheterocy
On the stereochemistry of 1,4-diheterocyclanes. IV—carbon-13 NMR spectra and structural properties of 1,4-dioxane-2,3-diols and their methyl-substituted derivatives
✍ Pertti Äyräs 📂 Article 📅 1978 🏛 John Wiley and Sons 🌐 English ⚖ 463 KB

## Abstract The 1,4‐dioxane‐2,3‐diols and a number of their methyl‐substituted derivatives were synthesized and their ^13^C NMR spectra measured. The configurational properties were studied on the basis of the spectral data and chemical equilibration. For the parent compound the __trans__ configura