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Rhodium-catalysed intramolecular trans-bis-silylation of alkynes to synthesise 3-silyl-1-benzosiloles

✍ Scribed by Matsuda, Takanori; Ichioka, Yoichiro

Book ID: 118177861
Publisher: Royal Society of Chemistry
Year: 2012
Tongue: English
Weight: 132 KB
Volume: 10
Category: Article
ISSN: 1477-0520
DOI: 10.1039/c2ob25242b

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Rh(l)-catalysed hydrocarbonylation of alkynes 1 in the presence of primary amines gives substituted 2-pyrrolidinones 3 in a one-pot procedure. Replacement of hydrogen by hydrosilanes via silylcarbonylation leads to 4-silylated 1-aza-1,3-butadienes 5. These azadienes are converted with dimethyl acety

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Corrigendum to the paper “Bis(di-t-butylphosphino) methane complexes of rhodium: homogeneous alkyne hydrosilylation by catalyst-dependent alkyne insertion into RhSi or RhH bonds. Molecular structures of the dimer [(dtbpm)RhCl]2 and of the silyl complex (dtbpm) Rh[Si(OEt)3](PMe3)” [J. Organomet. Chem., 490 (1995) 51–70]

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