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Rhodium-103 NMR of Carboxylate and Thiolate Complexes by Indirect Detection using Phosphorus

โœ Scribed by Laurence Carlton

Publisher
John Wiley and Sons
Year
1997
Tongue
English
Weight
282 KB
Volume
35
Category
Article
ISSN
0749-1581

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Natural abundance nitrogen-15 NMR spectr
Natural abundance nitrogen-15 NMR spectroscopy of rhodium complexes by indirect detection using phosphorus
โœ Laurence Carlton; Rosemarie Weber ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 251 KB ๐Ÿ‘ 2 views

Nitrogen-15 NMR spectra of the complexes and ] , each containing 15N at natural abundance, were obtained by indirect detection (HMQC) using phosphorus as the observed nucleus. Data collection times varied from 4 h to 4 d depending upon the accuracy of the estimated value of 2J(31P,15N) used to opti