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Resolution of salbutamol enantiomers in human urine by reversed-phase high performance liquid chromatography after derivatization with (S)-(-)-α-methylbenzyl isocyanate

✍ Scribed by Kyeong Ho Kim; Tae Kyun Kim; Young Hee Kwon; Young Taek Sohn

Publisher
Springer
Year
1997
Tongue
English
Weight
360 KB
Volume
20
Category
Article
ISSN
0253-6269

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Indirect resolution of baclofen enantiom
Indirect resolution of baclofen enantiomers from pharmaceutical dosage form by reversed-phase liquid chromatography after derivatization with Marfey's reagent and its structural variants
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A high-performance liquid chromatographic (HPLC) method was developed for chiral assay of baclofen enantiomers in pharmaceutical formulations using an indirect approach. Baclofen enantiomers were derivatized with Marfey's reagent (FDNP-L-Ala-NH 2 ) and its structural variants FDNP-L-Phe-NH 2 , FDNP-