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Research on african medicinal plants -XXV- the (1R,2S) absolute configuration of nyasicoside. Its occurrence in curculigorecurvata.

✍ Scribed by Kusamba Chifundera; I. Messana; C. Galeffi; Y. De Vicente


Publisher
Elsevier Science
Year
1991
Tongue
French
Weight
319 KB
Volume
47
Category
Article
ISSN
0040-4020

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✦ Synopsis


The (I$ configuration at C-l of nyasicoside and its derivatives was assigned by comparison of the Cotton effect with those of optically active phenylcarbinols, whereas the (2) configuration at C-2 was assigned by the application of the CD exciton chirality method for the dial his pbromobenzoates. Nyasicosidel, 1, is a monoglucoside of 1,5-bis(3',4'-dihydroxyphenyl)-1,2dihydroxy-pentan-4-yne isolated together with hypoxoside2, nyasoside3, mono-* Chemical shift values in ppm. 4 in CD30D, S-2 in CDC13. a, b, c, d These signals may be interchanged in the same column.