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Relationship between Dominant Conformation and Diastereoselectivity ofO-Acetal Formation of Saturated 2H-3,1-Benzothiazine-2-thiones

✍ Scribed by Perjési, Pál ;Batta, Gyula

Publisher
Wiley (John Wiley & Sons)
Year
1993
Tongue
English
Weight
220 KB
Volume
126
Category
Article
ISSN
0009-2940

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✍ Perjési, Pál ;Földesi, András ;Batta, Gyula ;Tamás, József 📂 Article 📅 1989 🏛 Wiley (John Wiley & Sons) 🌐 English ⚖ 523 KB

The reaction of 2-arylidenecyclohexanones 1 with dithiocarbamic acid gave three of the four possible diastereomers of 4-aryl-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2( 1 H)thiones 2-4. The isomeric composition of the reaction products was found to depend on the quantity of hydrochlor