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Regioselective addition of aniline to 8H-pyrido[2,3,4-mn]acridinone: structure determination of the reaction product

✍ Scribed by N. Fixler; M. Demeunynck; M. C. Brochier; J. Garcia; J. Lhomme

Publisher: John Wiley and Sons
Year: 1997
Tongue: English
Weight: 247 KB
Volume: 35
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(199711)35:10<697::aid-omr156>3.0.co;2-m

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✦ Synopsis

A combination of NMR techniques, including 13C and 1H DEPT, HMQC and HMBC experiments, was used to assign the structure of the compound formed by addition of aniline to 8H-pyrido [ 2,3,4-mn ] acridine. From this NMR study, two structures were possible. This ambiguity was removed by regioselective introduction of one deuterium on the starting compound. 1997

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