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Regio-, Diastereo-, and Enantioselective Synthesis ofvic-Diols via α-Silyl Ketones According to the SAMP/RAMP Hydrazone Method

✍ Scribed by Enders, Dieter ;Nakai, Shiro

Publisher
Wiley (John Wiley & Sons)
Year
1991
Tongue
English
Weight
828 KB
Volume
124
Category
Article
ISSN
0009-2940

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Regio-, Diastereo-, and Enantioselective
Regio-, Diastereo-, and Enantioselective Synthesis of Vicinal Diols via α-Silyl Ketones
✍ Dieter Enders; Shiro Nakai 📂 Article 📅 1990 🏛 John Wiley and Sons 🌐 German ⚖ 258 KB

A new versatile and efficient regio-, diastereo-, and enantioselective synthesis of vicinal diols s-trans-4, s-trans-5, and s-cis-4 is described. Symmetrical ketones are converted into their SAMP-or RAMP-hydrazones which are then silylated with (isopropy1oxy)dimethylsilyl chloride, followed by ozono