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Refocussing of chemical and paramagnetic shift anisotropies in 2H NMR using the quadrupolar-echo experiment

✍ Scribed by Sasa Antonijevic; Stephen Wimperis

Book ID
108487844
Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
239 KB
Volume
164
Category
Article
ISSN
1090-7807

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The 2D QUADSHIFT experiment: Separation
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## Abstract The two‐dimensional QUADSHIFT experiment is introduced, which permits the separation of chemical shifts and quadrupolar couplings in solid‐state magic angle spinning NMR spectra of powder samples. The technique was applied to partially deuteriated norcamphor and camphor under slow magic