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Reductive transformations, 20. Synthesis ofn-alkyl-substituted perylenes and terrylenes via alkali-metal induced cyclization of oligonaphthylenes

✍ Scribed by Anton, Ute ;Göltner, Christine ;Müllen, Klaus


Publisher
Wiley (John Wiley & Sons)
Year
1992
Tongue
English
Weight
724 KB
Volume
125
Category
Article
ISSN
0009-2940

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✦ Synopsis


Perylene / Terrylene / buy-Substitution / Steric strain The synthesis of two novel n-alkyl-or aryl-substituted perylenes and of an n-alkylated terrylene is possible by an alkalimetal induced cyclization of the corresponding bi-or trinaphthyls. Differences in reactivity of the naphthylenes in the ring-closure reaction are caused by the different substitution pattern. UV and fluorescence spectra as well as the stability of the resulting rylenes[*] are discussed as a function of substitution.