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Reductive Reactivity of the Organolanthanide Hydrides, [(C 5 Me 5 ) 2 LnH] x , Leads to ansa -Allyl Cyclopentadienyl (η 5 -C 5 Me 4 CH 2 −C 5 Me 4 CH 2 -η 3 ) 2- and Trianionic Cyclooctatetraenyl (C 8 H 7 ) 3- Ligands

✍ Scribed by Evans, William J.; Schmiege, Benjamin M.; Lorenz, Sara E.; Miller, Kevin A.; Champagne, Timothy M.; Ziller, Joseph W.; DiPasquale, Antonio G.; Rheingold, Arnold L.

Book ID: 126842304
Publisher: American Chemical Society
Year: 2008
Tongue: English
Weight: 276 KB
Volume: 130
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja8011726

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## Abstract The monoalkyl complexes [Zr{Me~2~Si(η^5^‐C~5~Me~4~)(η^5^‐C~5~H~3~R)}(R′)Cl] [R = Me, R′ = CH~2~Ph (1); R = Me, R′ = CH~2~SiMe~3~ (2); R = __i__Pr, R′ = CH~2~Ph (3); R = __i__Pr, R′ = CH~2~SiMe~3~ (4); R = SiMe~3~, R′ = CH~2~Ph (5); R = SiMe~3~, R′ = CH~2~SiMe~3~ (6)] have been synthesiz