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Reductive N Alkylation of Cyclo[8]pyrroles

✍ Scribed by Thomas Köhler; Zhongping Ou; Jeong Tae Lee; Daniel Seidel; Vincent Lynch; Karl M. Kadish; Jonathan L. Sessler

Publisher
John Wiley and Sons
Year
2004
Tongue
English
Weight
201 KB
Volume
117
Category
Article
ISSN
0044-8249

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Reductive N Alkylation of Cyclo[8]pyrrol
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✍ Thomas Köhler; Zhongping Ou; Jeong Tae Lee; Daniel Seidel; Vincent Lynch; Karl M 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 201 KB 👁 1 views

## Cyclo[8] pyrrole (1), although lacking bridging meso carbon atoms, may be considered as a larger analogue of porphyrin (2) in that it is flat and aromatic (see Scheme 1). [1] For this reason, we have been interested in exploring the chemical behavior of cyclo [8]pyrrole and contrasting it to th

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✍ Mihai Buda; Adriana Iordache; Christophe Bucher; Jean-Claude Moutet; Guy Royal; 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 452 KB

## Abstract Cyclo[8]pyrrole was obtained efficiently when 3,3′,4,4′‐tetraethylbipyrrole was subjected to bulk electrolysis, with yields spanning a range from close to 0 % with tetra‐__n__‐butylammonium fluoride as the electrolyte, to almost 70 % when tetra‐__n__‐butylammonium hydrogensulfate was us

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Electrochemically generated tetraethylammonium peroxy-corresponding N-alkylated pyrroles in high yields. C-Alkylated pyrroles have not been isolated in any case dicarbonate (TEAPC) and tetraethylammonium carbonate (TEAC) react under very mild conditions with pyrroles reported. affording, after addit