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Reductive dimerization of imines in a Pb/Al bimetal redox system

✍ Scribed by Hideo Tanaka; Hamid Dhimane; Hiroyuki Fujita; Youichi Ikemoto; Sigeru Torii

Publisher: Elsevier Science
Year: 1988
Tongue: French
Weight: 222 KB
Volume: 29
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)82121-8

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A novel mono and/or double allylation of acetals is achieved by the action of ally1 bromide, aluminium metal, and a catalytic amount of PbBr2 and A1Br3 in tetrahydrofuran.

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An electroreductive "Barbier Type" allylation of imines with ally1 bromide has been performed in a PbBqJ3uqNBqTI-G(Al anode)-(Pt cathode) system. A combination of Pb(O)/Pb(II) redox and a sacrificial aluminum anode works as a mediator for both cathodic and anodic electron transfer processes, respect

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Barbier Type" allylation of imines with ally1 bromide has been performed successfully by the action of aluminum (1 equiv.) and titanium(W) chloride (0.05 equiv.) in THF. The chirality transfer of a-amino acid esters to homoallyl amines is demonstrated by allylation of N-benzalvaline methyl ester fol

ChemInform Abstract: Reductive Cross-Cou

ChemInform Abstract: Reductive Cross-Coupling of 3-Substituted Δ3-Cephems with Alkenyl Halides in an Al/PbBr2/NiBr2(bpy) Triplemetal Redox System. Synthesis of 3-Alkenyl-Δ3-cephems.

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