Reductive Couplings of Ketones by Low-Valent Titanium, Prepared from TiCl4 and Reducing Agents
โ Scribed by R. Dams; M. Malinowski; H. J. Geise
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 2010
- Weight
- 405 KB
- Volume
- 90
- Category
- Article
- ISSN
- 0037-9646
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## Abstract A short and facile synthesis of a series of 1, 2โdihydroquiazolinโ4(3H)โones was accomplished in good yields via novel reductive cyclization of oโnitrobenzamides with ketones promoted by TiCl~4~/Zn system. The structure was established on the basis of elemental analysis, IR, 'H NMR and
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