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Reduction of vanadium(V) with ascorbic acid and isolation of the generated oxovanadium(IV) species

✍ Scribed by E. G. Ferrer; E. J. Baran

Book ID: 111636145
Publisher: Humana Press Inc
Year: 2001
Tongue: English
Weight: 126 KB
Volume: 83
Category: Article
ISSN: 0163-4984
DOI: 10.1385/bter:83:2:111

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## Abstract The reactions of V^V^O(O‐__i__Pr)~3~ with [PS3′]H~3~ and [PS3]H~3~ {[PS3′]H~3~ = P(C~6~H~3~‐5‐Me‐2‐SH)~3~, [PS3]H~3~ = P(C~6~H~4~‐2‐SH)~3~} led to the formation of [V^IV^(L)] [L = P2S4′ (1a), P2S4 (1b)], where L was formed by the oxidative coupling of two PS3′ or PS3 ligands by a disulf