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REDUCTION OF THE STEREOISOMERIC 4-ENOL METHYL ETHERS OF 1,4-DIMESITYL-1,2,4-BUTANETRIONE

✍ Scribed by LUTZ, ROBERT E.; TERRY, DANIEL H.

Book ID: 120274301
Publisher: American Chemical Society
Year: 1942
Tongue: English
Weight: 444 KB
Volume: 07
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01198a004

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## Abstract Methylation of ethyl 2, 4‐dioxopentanoate with diazomethane gives a mixture of two enol ethers, the 2‐methoxy and the 4‐methoxy isomer, with a product ratio which depends upon reaction temperature. Both enol ethers, initially (__Z__)‐configurated, isomerize to the corresponding (__E__)‐