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Reduction of 2-methyl β-carboline anhydronium base by sodium borohydride

✍ Scribed by I. W. Elliott


Book ID
112121485
Publisher
Journal of Heterocyclic Chemistry
Year
1966
Tongue
English
Weight
115 KB
Volume
3
Category
Article
ISSN
0022-152X

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## Abstract [^14^C]Methane (440 mCi) was prepared using the reduction of [^14^C]methyl iodide by sodium borohydride in diglyme in quantitative yield. The diborane formed was trapped as nonvolatile 9‐BBN. [^14^C]Methane free of any accompanying gases was conveniently distributed into calibrated glas