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Reduction and Re-Oxidation Behavior of Calcium Iron Phosphate, Ca9Fe(PO4)7.

✍ Scribed by B. I. Lazoryak; A. A. Belik; R. N. Kotov; I. A. Leonidov; E. B. Mitberg; V. V. Karelina; D. G. Kellerman; S. Yu. Stefanovich; A. K. Avetisov

Publisher: John Wiley and Sons
Year: 2003
Weight: 58 KB
Volume: 34
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200316014

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## Abstract A single crystal of the new title compound is synthesized in a flux of Rb~2~Mo~2~O~7~ from a starting mixture of Rb~2~CO~3~, Fe(NO~3~)~3~, (NH~4~)~2~HPO~4~, and MoO~3~ (Pt crucible, 473, 673, and 873 K for 24 h at each temperature).