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Redetermination of rhodanine at 173 K

✍ Scribed by Ng, Seik Weng

Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 72 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536807007374

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✦ Synopsis

The crystal structure of the title compound, C~3~H~3~NOS~2~, has been redetermined at 173 K. The geometric parameters show a significant improvement in precision from the orginal determination [Van der Helm, Lessor & Merritt (1962). Acta Cryst. 15, 1227–1232], where the data were measured using photographic film. In the crystal structure, molecules form planar N—H...S hydrogen-bonded dimers.

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