Redetermination of CaB8O11(OH)4 at low temperature
โ Scribed by Wiggin, Seth B. ;Weller, Mark T.
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 205 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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A low-temperature redetermination of metaldehyde (systematic name: 2,4,6,8-tetramethyl-1,3,5,7-tetroxocane), (CH 3 -CHO) 4 or C 8 H 16 O 4 , is reported, 69 years after the original determination [Pauling & Carpenter (1936). J. Am. Chem. Soc. 58, 1274Soc. 58, -1278]]. Metaldehyde crystallizes in the
The crystal structure of the title compound, (I), indole-3-carboxaldehyde was refined to R(F) = 0.053 from room-temperature diffraction measurements (Golubev & Kondrashev, 1984). This re-refinement represents an improvement; all H atoms were located and refined. In the crystal structure, the molecul