Redetermination of bis(2,2′-bipyridine-κ2N,N′)iodocopper(II) iodide
✍ Scribed by Liu, Yu ;Xu, Duan-Jun ;Wu, Jing-Yun ;Chiang, Michael Y.
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 219 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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The title compound, [CuCl 2 (C 10 H 8 N 2 )], has twofold symmetry and the coordination geometry around the Cu II atom is distorted square-planar. There are weak intermolecular CuÁ Á ÁCl interactions, forming a chain structure in the crystal.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.025 wR factor = 0.067 Data-to-parameter ratio = 15.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.008 A Ê R factor = 0.052 wR factor = 0.118 Data-to-parameter ratio = 12.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.008 A Ê Disorder in main residue R factor = 0.057 wR factor = 0.134 Data-to-parameter ratio = 15.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.