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Reassignment, Isolation, Spectral and X-ray Characterization of Diastereoisomers of the Macrocyclic Ligand 3,10-meso-3,5,7,7,10,12,14,14-Octamethyl-1,4,8,11-tetraazacyclotetradecane and their NiII and CuII Complexes

✍ Scribed by Yung-Chan Lin; Tarun Kumar Misra; Tian-Huey Lu; Maddirala Shambabu Joseph; Chung-Sun Chung

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
211 KB
Volume
2006
Category
Article
ISSN
1434-1948

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## Abstract The molecular structures of the title compounds 3 and 5 were investigated by NMR and X‐ray structural methods. The NMR results suggest two equivalent halves for both molecules. The X‐ray study shows an approximate mirror plane for 3 and an approximate twofold axis for a significant port