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Rearrangements of substituted 3-azidoazetidines: Unexpected formation of a substituted oxazole

✍ Scribed by Alan P. Marchand; D. Rajagopal; Simon G. Bott

Book ID
112131344
Publisher
Journal of Heterocyclic Chemistry
Year
1995
Tongue
English
Weight
182 KB
Volume
32
Category
Article
ISSN
0022-152X

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2-en-1-a1 ( l a ) 121, 4-(dimethylamino)but-3-en-2-one (lb) 131, and methyl 3-(dimethylamino)acrylate (Ic) [41 leads almost quantitatively t o the hydrobromides (2). which react with triethylamine t o give the bromine derivatives (3) in yields of more than 90 % [51. The acetylenes (4) are obtained f