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Rearrangement of unsaturated cyclic peroxides obtained by photooxygenation of 2,3-dimethylene-7-oxabenzonorbornene and 2,3-dimethylene-1,4-etheno-1,2,3,4-tetrahydronaphthalene

✍ Scribed by Recep Özen; Fatma Kormalı (Bayramoğlu); Metin Balci; Basri Atasoy

Book ID
108371324
Publisher
Elsevier Science
Year
2001
Tongue
French
Weight
153 KB
Volume
57
Category
Article
ISSN
0040-4020

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A concise synthesis of the 2,3-dimethylene-1,4-methano-1,2,3,4-tetrahydronaphthalene and its reaction with singlet oxygen
✍ Basri Atasoy; Fatma Bayramoğlu; Tuncer Hökelek 📂 Article 📅 1994 🏛 Elsevier Science 🌐 French ⚖ 781 KB

Palladium-catalyzed carbomethoxylation of benzonorbornadiene (7) yielded dimethyl-1.4methano-l,2.3.4-tetrahydronaphthalene-2,3-dicarboxylate (9) which was transformed in three steps into 2.3-dimethylene-l,4-methano-l.2,3.4-tetrahydronaphthalene (4) in a high yield. Reaction of 4 with singlet oxygen