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Reactivity of malononitrile towards sulphamide and N-substituted sulphamides: synthesis and hydrolysis reactions of 3,5-diamino-1,2,6-thiadiazine 1,1-dioxides

✍ Scribed by Alkorta, Ibon; Ar�n, Vicente J.; Bielsa, Agust�n G.; Stud, Manfred


Book ID
120665323
Publisher
Royal Society of Chemistry
Year
1988
Weight
576 KB
Volume
5
Category
Article
ISSN
1472-7781

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Alkyl and aryl N-substituted 1,2,5-thiadiazolidine and 1,2,6-thiadiazinane 1,1-dioxides 6 were synthesized in good yields from the reaction of sulfuryl chloride with 2-chloroethylamine or 3-chloropropylamine hydrochlorides, respectively, followed by treatment with a primary amine and triethylamine,