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Reactivity of Baccatin III Derivatives towards Samarium II reagents

✍ Scribed by Sandrine Py; Françoise Khuong-Huu

Book ID
103402406
Publisher
Elsevier Science
Year
1995
Tongue
French
Weight
237 KB
Volume
36
Category
Article
ISSN
0040-4039

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The reaction of 2,3,4,5-tetramethylphospholylpotassium alkyl complexes [(C 4 Me 4 P) 2 LnCH(SiMe 3 ) 2 ]; these complexes were most efficiently prepared from [LnCl 3 (THF) x ], [C 4 Me 4 PK] with [LnCl 3 (THF) x ] (Ln = Nd, Sm) in a 2:1 ratio gave unsolvated ate complexes of the formula [KC 4 Me 4 P