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Reactions with Heterocyclic Arylazo Compounds: Synthesis of New 1-Azoloylimidazolones

✍ Scribed by Hassan A. Elfahham; Ibraheim Elsakka; Nadia R. Mohamed; Mohamed H. Elnagdi

Publisher: John Wiley and Sons
Year: 1983
Tongue: English
Weight: 162 KB
Volume: 316
Category: Article
ISSN: 0365-6233
DOI: 10.1002/ardp.19833160912

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## Experimental Section DMP (2.0 equiv) was added in one portion to a solution of 7 a (0.1 mmol) in benzene (4 mL) or BTF. [6] The solution was heated at reflux (or at 80 ± 85 8C for the reactions in BTF) for about 30 min at which point TLC indicated complete consumption of starting material. Dilu