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Reactions of chloromethyl iso(thio)cyanato(thio)phosphonates with 1,2-diaminocyclohexane

✍ Scribed by M. A. Pudovik; R. Kh. Bagautdinova

Book ID: 111459914
Publisher: Springer
Year: 2008
Tongue: English
Weight: 137 KB
Volume: 78
Category: Article
ISSN: 1070-3632
DOI: 10.1134/s1070363208120189

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Reactions o f phenyl isothiocyanato (di) chloromethyl(thio)phosphonates (1) with thiols in the presence of a base give rise to 2-alkylthio-4,5-dihydro-4oxo(th ioxo)-4-phenoxy-I ,3,4-th iazaphospholes (5). Some of these compounds can also be obtained by alkylation o f 2,4-dithioxo-4-phenoxy-l,3,4-thi