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Reactions of 4-chloromethyl-1,3,2-dioxathiolane 2-oxides with sodium phenoxide. A reinvestigation

✍ Scribed by Z. A. Bredikhina; A. V. Pashagin; A. A. Bredikhin

Publisher: Springer
Year: 2000
Tongue: English
Weight: 286 KB
Volume: 49
Category: Article
ISSN: 1573-9171
DOI: 10.1007/bf02496348

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## Abstract In contrast to previous reports, 4‐ethoxy‐1,1,1‐trifluoro‐3‐buten‐2‐one (**1**) was observed to react with methylhydrazine (**2**) in refluxing ethanol to yield 1‐methyl‐3‐(trifluoromethyl)pyrazole (**6**) and 4,5‐dihydro‐1‐methyl‐5‐(trifluoromethyl)pyrazol‐5‐ol (**4**). The later compo