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Reactions of 2,3-diphenylthiirene 1,1-dioxide with nucleophiles

✍ Scribed by Jarvis, Bruce B.; Stahly, G. Patrick

Book ID: 120938711
Publisher: American Chemical Society
Year: 1980
Tongue: English
Weight: 847 KB
Volume: 45
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01301a013

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## Abstract __N__‐Silylated 3‐acetoxy‐1,2‐thiazetidine 1,1‐dioxide (5) is prepared from L‐cystine. Reactions of 5 with silyl enol ethers yield C‐3‐substituted β‐sultams 6, 12 and 15. Desilylation of 6 affords 7, which undergoes photochemical cyclization to give the bicyclic β‐sultam 10. In the cour