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Reactions of 13CO with Ethoxycarbonylcarbene-Bridged Dicobalt Carbonyl Complexes: [μ2-{Ethoxycarbonyl(methylene)}-μ2-(carbonyl)bis(tricarbonylcobalt)(Co–Co)] and [Di-μ2-{ethoxycarbonyl(methylene)}bis(tricarbonylcobalt)(Co–Co)]

✍ Scribed by Eszter Fördős; Neszta Ungvári; Tamás Kégl; Ferenc Ungváry

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
118 KB
Volume
2006
Category
Article
ISSN
1434-1948

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✍ W. Petz; F. Weller; A. Barthel; C. Mealli; J. Reinhold 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 German ⚖ 253 KB 👁 1 views

The reaction of Na 2 [Fe(CO) 4 ] with Br 2 CF 2 in npentane generates a mixture of the compounds (CO) 3 Fe(l-CO) 3±n (l-CF 2 ) n Fe(CO) 3 (2, n = 2; 3, n = 1) in low yields with 3 as the main product. 3 is obtained free from 2 by reacting Br 2 CF 2 with Na 2 [Fe 2 (CO) 8 ]. The non-isolable monomeri