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Reaction of Thiaxanthydrol With Compounds Containing Active Hydrogen

✍ Scribed by SAWICKI, EUGENE.; OLIVERIO, VINCENT T.

Book ID: 126993052
Publisher: American Chemical Society
Year: 1956
Tongue: English
Weight: 682 KB
Volume: 21
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01108a009

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## Abstract While 4‐chloroxanthione **1** gives with diazomethane the dithiol **2**, it reacts with other diazoalkanes to give the episulfides **3**–**5**, desulfurization of which forms the ethylenes **6** and **7**. Malononitrile and ethyl cyanoacetate react with **1** to give the cyano derivativ