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Reaction of [{PhP(Se)(μ-Se)}2] with Dialkyl Cyanamides: X-ray Crystal Structures of the Phosphorus-Containing Triselenapentalenes [Me2N−C(Se)=N]2P(Se)Ph and [O(CH2CH2)2N−C(Se)=N]2P(Se)Ph

✍ Scribed by Pravat Bhattacharyya; Alexandra M. Z. Slawin; J. Derek Woollins

Publisher: John Wiley and Sons
Year: 2000
Tongue: English
Weight: 110 KB
Volume: 112
Category: Article
ISSN: 0044-8249
DOI: 10.1002/1521-3757(20000602)112:11<2049::aid-ange2049>3.0.co;2-j

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The ligands [Ph 2 (S)PNHP(X)Ph 2 ] -(X = O, Se) react with InCl 3 coordination geometry in 2 resembles that observed in the three analogous tris-chelates incorporating the corres-in a 3:1 ratio to give a tris-chelate [In{Ph 2 P(O)NP(S)Ph 2 -O,S} 3 ]•0.75 C 6 H 6 (2) and the unexpected pentacoordinat