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Reaction of nitrosobenzene with 1,2,3,4-tetrachloro-5,5-ethylenedioxycyclopentadiene

✍ Scribed by P.M. Adler; R.J. Bennet; Janet Fieldman; G.I. Fray

Publisher
Elsevier Science
Year
1978
Tongue
French
Weight
219 KB
Volume
34
Category
Article
ISSN
0040-4020

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## Abstract A synthesis of C‐chlorinated analogues of 1,5‐diaza‐2,4‐diphosphorinan‐6‐ones is described. The P‐chlorophosphine 3, a key compound for all reported substitution reactions, reacts in an unusual way with N,N′‐dimethyl‐N,N′‐bis(trimethylsilyl)urea to give the unsymmetrical product 5, the