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Reaction of Lead Soaps with Sodium Iodide

โœ Scribed by Barnett, Robert S.


Book ID
126082391
Publisher
American Chemical Society
Year
1946
Weight
167 KB
Volume
18
Category
Article
ISSN
0096-4484

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Orthanilic acid from the reaction of o-n
โœ A. Wagenaar; Jan B.F.N. Engberts ๐Ÿ“‚ Article ๐Ÿ“… 1973 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 109 KB

We wish to report a novel redox reaction in which o\_nitrobenzenesulfinic acid (1) is transformed into orthanilic acid (2). Thus, reaction of 1 with six equivalents of sodium iodide in ethanol at 70' for 17 hours afforded' 2\_ (4%) as the major product while the other products identified were g-iodo