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Reaction of isothiourea with 2,3-diaza-3-pentenedioic anhydride. A solid-phase synthesis of 3-amino-1,2,4-triazin-5(4H)-ones

✍ Scribed by Rui-Yang Yang; Alan P Kaplan

Publisher: Elsevier Science
Year: 2001
Tongue: French
Weight: 113 KB
Volume: 42
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)00766-3

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✦ Synopsis

The first reported solid-phase synthesis of 3-amino-1,2,4-triazin-5(4H)-ones is described. Reactions of polymer-bound isothiourea with 2,3-diaza-3-pentenedioic anhydride forms 3-amino-1,2,4-triazin-5(4H)-ones in good yields and high purity.

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