The reaction of dibenzalcyclohexanone with hydroxylamine hydrochloride affords three compounds: the oxime of 2-benzylidenecyclohexanone (Z), 3-phenyl-7-benzylidene-3,3a,4,5,6,7-hexahydr~2,l-ben~soxazole (3) and 3-phenyl-3,3a,4,5,6,7-hexahydro-2,l-ben~soxazol~7~pir~~~~-phenylaziridine) (4). Their str
Reaction of dibenzalacetone with hydroxylamine hydrochloride under phase-transfer conditions. 1H and 13C 2D NMR structural elucidation of the products
✍ Scribed by J. L. Aguilera; G. Sosa; W. F. Reynolds; E. Diaz; H. Barrios
- Publisher
- John Wiley and Sons
- Year
- 1989
- Tongue
- English
- Weight
- 450 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
The constitution, configuration and conformation of three N-hydroxydiphenylpiperidines were established by 'H and 13C 2D NMR spectroscopy. The products were obtained using phase-transfer conditions.
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