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Reaction of CpW(CO) 2 (μ-PPh 2 )Mo(CO) 5 and Fe 2 (μ-S 2 )(CO) 6 : Unusual Fragmentation and Coordination of Fe 2 (μ-S 2 )(CO) 6

✍ Scribed by Hossain, Md. Munkir; Lin, Hsiu-Mei; Shyu, Shin-Guang

Book ID
121867869
Publisher
American Chemical Society
Year
2004
Tongue
English
Weight
212 KB
Volume
23
Category
Article
ISSN
0276-7333

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The reaction of Na 2 [Fe(CO) 4 ] with Br 2 CF 2 in npentane generates a mixture of the compounds (CO) 3 Fe(l-CO) 3±n (l-CF 2 ) n Fe(CO) 3 (2, n = 2; 3, n = 1) in low yields with 3 as the main product. 3 is obtained free from 2 by reacting Br 2 CF 2 with Na 2 [Fe 2 (CO) 8 ]. The non-isolable monomeri