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Reaction of bisdiazo ketones with acrylonitrile

✍ Scribed by A. L. Fridman; G. S. Ismagilova; V. S. Zalesov; N. A. Kolobov; V. V. Larikov

Book ID
112441505
Publisher
Springer US
Year
1973
Tongue
English
Weight
81 KB
Volume
9
Category
Article
ISSN
0009-3122

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Baylis–Hillman reactions of N-arylidened
Baylis–Hillman reactions of N-arylidenediphenylphosphinamides with methyl vinyl ketone, methyl acrylate, and acrylonitrile
✍ Min Shi; Gui-Ling Zhao πŸ“‚ Article πŸ“… 2002 πŸ› Elsevier Science 🌐 French βš– 70 KB

We have found that in the Baylis-Hillman reactions of N-arylidenediphenylphosphinamides 1 with methyl vinyl ketone (MVK), methyl acrylate or acrylonitrile, the Lewis base and solvent can significantly affect the reaction rate. Using PPh 3 as Lewis base in the reaction of 1 with MVK in DMF, THF or Me