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Reaction of acridinium salts with phenylhydrazones and phenylhydrazides

โœ Scribed by O. N. Chupakhin; I. Ya. Postovskii; V. L. Rusinov; V. N. Narushin


Book ID
112325127
Publisher
Springer US
Year
1975
Tongue
English
Weight
328 KB
Volume
11
Category
Article
ISSN
0009-3122

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residue remaining on evaporation was chromatographed on 850 g of silica gel (column 4x90 cm) with hexane/acetone (100: 3). The first 300 ml of eluate contained 10.9 g of crude product (30). This was taken up in ether, and washed with 1 % hydrochloric acid and 1 % sodium hydrogen carbonate solution;