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Reaction of acetals and orthoesters with decaborane and diacetonitrile decaborane

โœ Scribed by L. I. Zahkarkin; V. I. Stanko; Yu. A. Chapovskii

Book ID
112432163
Publisher
Springer
Year
1962
Tongue
English
Weight
156 KB
Volume
11
Category
Article
ISSN
1573-9171

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An efficient protection of carbonyls and
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โœ Seung Hwan Lee; Ji Hee Lee; Cheol Min Yoon ๐Ÿ“‚ Article ๐Ÿ“… 2002 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 350 KB

Carbonyls were efficiently converted to the corresponding dimethyl acetals at room temperature using trimethyl orthoformate and 1 mol% of decaborane under a nitrogen atmosphere. In turn, acetals were deprotected to the corresponding carbonyls using 1 mol% of decaborane in aqueous THF chemoselectivel