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Reaction of 3-cyanopyridine-2(1H)-thiones with N-butyllithium

✍ Scribed by N. G. Frolova; V. K. Zav'yalova; V. P. Litvinov

Publisher
Springer US
Year
1996
Tongue
English
Weight
272 KB
Volume
32
Category
Article
ISSN
0009-3122

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## Abstract magnified image Treatment of 1‐(2‐azidoarylmethyl)‐1__H__‐benzotriazoles (**6**) with __n__‐BuLi (2.5 equiv.) in THF at βˆ’78Β°C, followed by an addition of alkyl halides such as allyl, benzyl, and ethyl bromides with stirring for 2 h at room temperature afforded 2‐(dialkylamino)‐3‐(benzo