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Reaction of 3-chloro-1-(2,4,6-trimethylphenyl)propan-2-one with amines

✍ Scribed by R. R. Yadigarov; A. N. Khalilov; I. G. Mamedov; F. N. Nagiev; A. M. Magerramov; M. A. Allakhverdiev

Book ID
111465233
Publisher
SP MAIK Nauka/Interperiodica
Year
2009
Tongue
English
Weight
161 KB
Volume
45
Category
Article
ISSN
1070-4280

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ChemInform Abstract: Reaction of 3-Chlor
ChemInform Abstract: Reaction of 3-Chloro-1-(2,4,6-trimethylphenyl)propan-2-one with Amines.
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## Abstract The reaction of the title α‐chloro ketone (II) with primary amines is unexpectedly accompanied by a Favorskii rearrangement furnishing the amides (IV) (7 examples).

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.038 wR factor = 0.111 Data-to-parameter ratio = 13.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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View of the molecule of (I), showing the atom-labeling scheme. Displacement ellipsoids are drawn at the 30% probability level.